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10,11-Dihydro­dibenzo[b,f]azepine-5-carbothioic S-acid

✍ Scribed by Jin, Wei-Hua ;Jin, Can ;Hong, Zhi ;Wang, Ping

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
347 KB
Volume
62
Category
Article
ISSN
1600-5368

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✦ Synopsis

In the title molecule, C~15~H~13~NOS, the bond lengths and angles show normal values. No classical hydrogen bonds are found in the crystal packing, which is stabilized by van der Waals forces.

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✍ Roland Heckendorn 📂 Article 📅 1987 🏛 John Wiley and Sons 🌐 German ⚖ 532 KB

The stereoselectivity of the reduction of 5-carbamoyl-l0, I 1-dihydro-1 l-oxo-SH-dibenz[bflazepine-lO-yl acetate (6), prepared in two steps from 10, I l-dihydro-lO-oxo-5H-dibenz[hflazepine-5-carboxamide (4), has been studied. Among the reagents used, diisobutylaluminum hydride (DIBAH) was found to g