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5-Chloro­carbonyl-10,11-dihydro-5H-dibenz[b,f]azepine

✍ Scribed by Vijay, T. ;Anilkumar, H. G. ;Yathirajan, H. S. ;Narasimhamurthy, T. ;Rathore, R. S.

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
247 KB
Volume
61
Category
Article
ISSN
1600-5368

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The stereoselectivity of the reduction of 5-carbamoyl-l0, I 1-dihydro-1 l-oxo-SH-dibenz[bflazepine-lO-yl acetate (6), prepared in two steps from 10, I l-dihydro-lO-oxo-5H-dibenz[hflazepine-5-carboxamide (4), has been studied. Among the reagents used, diisobutylaluminum hydride (DIBAH) was found to g