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X-ray crystallographic characterization of 10,11-dihydro-5H-dibenz[b, f ]azepine-5-carboxamide

✍ Scribed by G. Bandoli; M. Nicolini; A. Ongaro; G. Volpe; A. Rubello

Publisher
Springer
Year
1992
Tongue
English
Weight
345 KB
Volume
22
Category
Article
ISSN
1572-8854

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The stereoselectivity of the reduction of 5-carbamoyl-l0, I 1-dihydro-1 l-oxo-SH-dibenz[bflazepine-lO-yl acetate (6), prepared in two steps from 10, I l-dihydro-lO-oxo-5H-dibenz[hflazepine-5-carboxamide (4), has been studied. Among the reagents used, diisobutylaluminum hydride (DIBAH) was found to g