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1-Methoxy­ethyl-5-nitro­benzimidazole

✍ Scribed by Akkurt, Mehmet ;Yıldırım, Sema Öztürk ;Orhan, Ersin ;Küçükbay, Hasan ;Büyükgüngör, Orhan

Publisher
International Union of Crystallography
Year
2005
Tongue
English
Weight
180 KB
Volume
61
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 10 H 11 N 3 O 3 , was synthesized by the reaction of 5-nitrobenzimidazole, 2-chloroethyl methyl ether and KOH in ethanol. The bond lengths and angles are unexceptional.

📜 SIMILAR VOLUMES

1-[2-(5-Nitro-1H-benzimidazol-1-yl)ethyl
1-[2-(5-Nitro-1H-benzimidazol-1-yl)ethyl]morpholinium chloride
✍ Akkurt, Mehmet ;Türktekin, Sevim ;Küçükbay, Hasan ;Yılmaz, Ülkü ;Büyükgüngör, Or 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 272 KB

Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.001 A Ê R factor = 0.027 wR factor = 0.069 Data-to-parameter ratio = 14.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

1-[2-(5-Nitro-1H-benzimidazol-1-yl)ethyl
1-[2-(5-Nitro-1H-benzimidazol-1-yl)ethyl]morpholinium chloride. Corrigendum
✍ Akkurt, Mehmet ;Türktekin, Sevim ;Küçükbay, Hasan ;Yılmaz, Ülkü ;Büyükgüngör, Or 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 37 KB

In the paper by Akkurt, Türktekin, Küçükbay, Yılmaz & Büyükgüngör [__Acta Cryst.__ (2005), E**61**, o166–o168], the experimental section is incorrect. The correct experimental section is given below.

1-(2-Bromo-1,1-di­methoxy­ethyl)-4-nitro
1-(2-Bromo-1,1-di­methoxy­ethyl)-4-nitro­benzene
✍ Shen, Yu-Dong ;Wu, Hai-Qiang ;Bu, Xian-Zhang ;Gu, Lian-Quan ;Ng, Seik Weng 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 214 KB

Methyl 4-nitrophenyl ketone was brominated by copper(II) bromide in methanol; the ketone reacts with the solvent in situ to yield the title compound, C 10 H 12 BrNO 4 , which exists as a monomeric molecule.

3-[(3-Ethyl-1-methyl-4-nitro-1H-pyrazol-
3-[(3-Ethyl-1-methyl-4-nitro-1H-pyrazol-5-yl)carbon­yl]-1H-benzimidazole
✍ Tan, Cheng-Xia ;Sun, Na-Bo ;Weng, Jian-Quan ;Shen, De-Long 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 114 KB

In the title compound, C~14~H~13~N~5~O~3~, the dihedral angle formed between the five-membered pyrazole and the benzimidazole ring system is 68.2 (2)°.

5-Nitro-1-(2-piperidinoeth­yl)-1H-benzim
5-Nitro-1-(2-piperidinoeth­yl)-1H-benzimidazole
✍ Akkurt, Mehmet ;Yıldırım, Sema Öztürk ;Küçükbay, Hasan ;Şireci, Nihat ;Fun, Hoon 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 190 KB

Single-crystal X-ray study T = 273 K Mean (C-C) = 0.005 A R factor = 0.072 wR factor = 0.219 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Aqua(5-nitro-1H-benzimidazole)(oxydiacet
Aqua(5-nitro-1H-benzimidazole)(oxydiacetato)copper(II)
✍ Zhang, Wan-Ju ;Li, Yan-Tuan ;Wu, Zhi-Yong 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 661 KB

In the molecule of the title compound, [Cu(C 4 H 4 O 5 )-(C 7 H 5 N 3 O 2 )(H 2 O)], the Cu II atom is coordinated by one tridentate oxydiacetate (ODA) dianion, one monodentate nitrobenzimidazole (NBZIM) molecule and one H 2 O molecule, in a distorted square-based pyramidal geometry. In the crystal