In the paper by Akkurt, Türktekin, Küçükbay, Yılmaz & Büyükgüngör [__Acta Cryst.__ (2005), E**61**, o166–o168], the experimental section is incorrect. The correct experimental section is given below.
1-[2-(5-Nitro-1H-benzimidazol-1-yl)ethyl]morpholinium chloride
✍ Scribed by Akkurt, Mehmet ;Türktekin, Sevim ;Küçükbay, Hasan ;Yılmaz, Ülkü ;Büyükgüngör, Orhan
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 272 KB
- Volume
- 61
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.001 A Ê R factor = 0.027 wR factor = 0.069 Data-to-parameter ratio = 14.3
For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
📜 SIMILAR VOLUMES
Single-crystal X-ray study T = 273 K Mean (C-C) = 0.005 A R factor = 0.072 wR factor = 0.219 Data-to-parameter ratio = 12.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
In the title compound, C~14~H~13~N~5~O~3~, the dihedral angle formed between the five-membered pyrazole and the benzimidazole ring system is 68.2 (2)°.
Single-crystal X-ray study T = 100 K Mean '(C±C) = 0.004 A Ê R factor = 0.025 wR factor = 0.056 Data-to-parameter ratio = 18.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
The title compound, C 10 H 11 N 3 O 3 , was synthesized by the reaction of 5-nitrobenzimidazole, 2-chloroethyl methyl ether and KOH in ethanol. The bond lengths and angles are unexceptional.