Single-crystal X-ray study T = 290 K Mean '(C±C) = 0.003 A Ê R factor = 0.027 wR factor = 0.062 Data-to-parameter ratio = 11.8 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
1-(2-Bromo-1,1-dimethoxyethyl)-4-nitrobenzene
✍ Scribed by Shen, Yu-Dong ;Wu, Hai-Qiang ;Bu, Xian-Zhang ;Gu, Lian-Quan ;Ng, Seik Weng
- Publisher
- International Union of Crystallography
- Year
- 2004
- Tongue
- English
- Weight
- 214 KB
- Volume
- 60
- Category
- Article
- ISSN
- 1600-5368
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✦ Synopsis
Methyl 4-nitrophenyl ketone was brominated by copper(II) bromide in methanol; the ketone reacts with the solvent in situ to yield the title compound, C 10 H 12 BrNO 4 , which exists as a monomeric molecule.
📜 SIMILAR VOLUMES
The title compound, C~7~H~3~BrNO~2~, was synthesized by the nitration of 1-bromo-2-(trifluoromethyl)benzene. In the crystal structure, there are three independent molecules, one of which lies on a crystallographic mirror plane.
The title compound, C 10 H 11 N 3 O 3 , was synthesized by the reaction of 5-nitrobenzimidazole, 2-chloroethyl methyl ether and KOH in ethanol. The bond lengths and angles are unexceptional.