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1-(2-Morpholinoethyl)-3-(3-phenyl­acryl­oyl)­thio­urea

✍ Scribed by Yamin, Bohari M. ;Hassan, Ibrahim N.

Book ID
104483051
Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
233 KB
Volume
60
Category
Article
ISSN
1600-5368

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✦ Synopsis

The title compound, C 16 H 21 N 3 O 2 S, is a thiourea derivative with cinnamoyl and 2-morpholinoethyl groups attached at the terminal two N atoms. The groups lie trans and cis, respectively, to the S atom across the thiourea CÐN bonds and the morpholine group adopts a chair conformation. The molecules are linked by NÐHÁ Á ÁO hydrogen bonds, forming an in®nite one-dimensional chain along the b axis.

📜 SIMILAR VOLUMES

1-(2-Chloro­benzo­yl)-3-phenyl­thio­urea
1-(2-Chloro­benzo­yl)-3-phenyl­thio­urea
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The phenyl and benzoyl groups in the title molecule, C~14~H~11~ClN~2~OS, are __cis__ and __trans__, respectively, with respect to the C=S bond. The molecular conformation is stabilized by an N—H...O hydrogen bond and the crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.

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1-(3-Chloro­benzo­yl)-3-methyl-3-phenyl­
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In the title compound, C~15~H~13~ClN~2~OS, the geometric parameters do not show unusual features. There are three molecules in the asymmetric unit. The molecules are linked by N—H...S hydrogen bonds to form dimers.

1-(3-Chloro­benzo­yl)-3-[3-(trifluoro­me
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✍ Khawar Rauf, M. ;Badshah, Amin ;Flörke, Ulrich 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 174 KB

## Single -crystal X-ray study T = 120 K Mean (C-C) = 0.004 A R factor = 0.057 wR factor = 0.120 Data-to-parameter ratio = 16.7 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.