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1-(2,2-Dimethyl­propion­yl)-3-phenyl­thio­urea

✍ Scribed by Yusof, M. Sukeri M. ;Ramadzan, Nurul 'Izzah A. ;Yamin, Bohari M.


Book ID
104488652
Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
272 KB
Volume
62
Category
Article
ISSN
1600-5368

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1-(2-Chloro­benzo­yl)-3-phenyl­thio­urea
✍ Khawar Rauf, M. ;Badshah, Amin ;Saeed, Aamer ;Bolte, Michael 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 107 KB

The phenyl and benzoyl groups in the title molecule, C~14~H~11~ClN~2~OS, are __cis__ and __trans__, respectively, with respect to the C=S bond. The molecular conformation is stabilized by an N—H...O hydrogen bond and the crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.

1-(2,3-Dimethyl­phen­yl)-3-(2-methyl­ben
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 168 KB

The benzoyl and dimethylphenyl groups in the title compound, C~17~H~18~N~2~OS, are __cis__ and __trans__, respectively, with respect to the C=S bond. The crystal packing is characterized by N—H...O and N—H...S hydrogen bonds.

1-(2,4-Dichloro­benzo­yl)-3-phenyl­thio­
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael ;Ahmad, Imtiaz 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 192 KB

The title compound, C~14~H~10~Cl~2~N~2~OS, crystallizes with two molecules in the asymmetric unit. The two molecules, differing only in the conformation of the dichlorophenyl ring, show the typical geometric parameters of substituted thiourea derivatives. The crystal packing is characterized by N—H.

1-Benzyl-3-(2-methyl­benzo­yl)thio­urea
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 198 KB

The dihedral angle between the benzoyl and benzyl groups in the title compound, C 16 H 16 N 2 OS, is 63.63 (4) . The crystal packing is characterized by N-HÁ Á ÁO and N-HÁ Á ÁS hydrogen bonds.

1-(3-Chloro­benzo­yl)-3-methyl-3-phenyl­
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael ;Ahmad, Imtiaz 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 133 KB

In the title compound, C~15~H~13~ClN~2~OS, the geometric parameters do not show unusual features. There are three molecules in the asymmetric unit. The molecules are linked by N—H...S hydrogen bonds to form dimers.