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μ-Oxalato-bis­[(1,4,8,11-tetra­azacyclo­tetra­decane)nickel(II)] bis­(perchlorate) hemihydrate

✍ Scribed by Liu, Hui ;Gu, Wu ;Tong, Xiao-Lan ;Kou, Ying-Ying ;Yan, Shi-Ping

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
135 KB
Volume
62
Category
Article
ISSN
1600-5368

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Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.004 A Ê Disorder in solvent or counterion R factor = 0.037 wR factor = 0.091 Data-to-parameter ratio = 15.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

Aqua­chloro(1,4,8,11-tetra­aza­un­decane
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The title compound, [NiCl(C 7 H 20 N 4 )(H 2 O)]Cl, has the Ni atom in a distorted octahedral coordination with the four amino N atoms occupying a square plane while the chloro and aqua ligands occupy the axial positions. The NiÐN bond distances range from 2.079 (1) to 2.088 (2) A Ê .