𝔖 Bobbio Scriptorium
✦   LIBER   ✦

[1,8-Bis(2-phenyl­ethyl)-1,3,6,8,10,13-hexa­aza­cyclo­tetra­decane]­nickel(II) bis­(tetra­fluoro­borate)

✍ Scribed by Li, Yan-Wu ;Xiang, Hua ;Lu, Tong-Bu ;Ng, Seik Weng

Publisher
International Union of Crystallography
Year
2004
Tongue
English
Weight
400 KB
Volume
60
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.004 A Ê Disorder in solvent or counterion R factor = 0.037 wR factor = 0.091 Data-to-parameter ratio = 15.0 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

📜 SIMILAR VOLUMES

[1,8-Bis(2-benzyl)-1,3,6,8,10,13-hexa­az
[1,8-Bis(2-benzyl)-1,3,6,8,10,13-hexa­aza­cyclo­tetra­decane]­nickel(II) diperchlorate
✍ Li, Yan-Wu ;Xiang, Hua ;Lu, Tong-Bu ;Ng, Seik Weng 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 383 KB

Single-crystal X-ray study T = 298 K Mean '(C±C) = 0.004 A Ê R factor = 0.036 wR factor = 0.105 Data-to-parameter ratio = 17.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

2,9-Bis­(methoxy­methyl)-1,3,8,10-tetra­
2,9-Bis­(methoxy­methyl)-1,3,8,10-tetra­thia­cyclo­tetra­decane
✍ Gültekin, Zeynep ;Bayrak, Hacer ;Frey, Wolfgang ;Hökelek, Tuncer 📂 Article 📅 2004 🏛 International Union of Crystallography 🌐 English ⚖ 243 KB

The title compound, C 14 H 28 O 2 S 4 , possesses a crystallographically imposed inversion centre and has two methine C atoms linked to methoxymethyl functional groups. It is in the exodentate conformation, with the four S atoms lying on the edges of the `rectangular' macrocycle. The lone pairs of e

cis-2,4,6,8-Tetra­nitro-1H,5H-2,4,6,8-te
cis-2,4,6,8-Tetra­nitro-1H,5H-2,4,6,8-tetra­aza­bi­cyclo­[3.3.0]­octane, the energetic compound `bi­cyclo-HMX'
✍ Gilardi, Richard ;Flippen-Anderson, Judith L. ;Evans, Robin 📂 Article 📅 2002 🏛 International Union of Crystallography 🌐 English ⚖ 304 KB

Single-crystal X-ray study T = 294 K Mean '(C±C) = 0.003 A Ê R factor = 0.036 wR factor = 0.091 Data-to-parameter ratio = 7.9 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.