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α-Pentafluoroethylated amines: a new synthetic approach

✍ Scribed by Martin H. Königsmann; Enno Lork; Irina L. Odinets; Valentine G. Nenajdenko; Nukolaj E. Shevchenko; Gerd-Volker Röschenthaler

Book ID
111730726
Publisher
Royal Society of Chemistry
Year
2006
Tongue
English
Weight
250 KB
Volume
16
Category
Article
ISSN
0959-9436

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✍ Dieter Enders; Reni Joseph; Christine Poiesz 📂 Article 📅 1998 🏛 Elsevier Science 🌐 French ⚖ 648 KB

N-BOC protected ct-hydrazinoketones 4 and N-tris protected ct-aminoketones 6 were synthesized in good overall yields by deprotonation and electrophilic amination of the corresponding ketone-N,N-dimethylhydrazones 2 and subsequent oxidative cleavage of the resulting product hydrazones 3 and 5 by ozon