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Zur Chemie des (2,4,6-Tri-tert-butylphenyl)isocyanids

✍ Scribed by Pakusch, Jeachim ;Rüchardt, Christoph

Publisher
Wiley (John Wiley & Sons)
Year
1989
Tongue
English
Weight
181 KB
Volume
122
Category
Article
ISSN
0009-2940

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✍ Ralf Riedel; Dr. Hans-Dieter Hausen; Prof. Dr. Ekkehard Fluck 📂 Article 📅 1985 🏛 John Wiley and Sons 🌐 English ⚖ 269 KB 👁 1 views

pounds, presumably oligomers. In glacial acetic acid (CH3C0,H/CH2C12=3 :2, i=40 mA/cm2, T=2OoC, Pt electrode) 17% androstanyl acetate is obtained and 38% androstane is recovered. Remarkable is the selectivity of the oxidation: We found that the 6-(6a), 7-, and 12-acetates are formed in the ratio 35