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Bis(2,4,6-tri-tert-butylphenyl)bicyclotetraphosphan

✍ Scribed by Ralf Riedel; Dr. Hans-Dieter Hausen; Prof. Dr. Ekkehard Fluck

Publisher
John Wiley and Sons
Year
1985
Tongue
English
Weight
127 KB
Volume
97
Category
Article
ISSN
0044-8249

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Bis(2,4,6-tri-tert-butylphenyl)bicyclote
Bis(2,4,6-tri-tert-butylphenyl)bicyclotetraphosphane
✍ Ralf Riedel; Dr. Hans-Dieter Hausen; Prof. Dr. Ekkehard Fluck πŸ“‚ Article πŸ“… 1985 πŸ› John Wiley and Sons 🌐 English βš– 269 KB

pounds, presumably oligomers. In glacial acetic acid (CH3C0,H/CH2C12=3 :2, i=40 mA/cm2, T=2OoC, Pt electrode) 17% androstanyl acetate is obtained and 38% androstane is recovered. Remarkable is the selectivity of the oxidation: We found that the 6-(6a), 7-, and 12-acetates are formed in the ratio 35