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Bis(2, 4, 6-tri-tert-butylphenyl)stannandiyl, ein Diarylstannylen ohne Donorstabilisierung

✍ Scribed by Prof. Dr. Manfred Weidenbruch; Josephin Schlaefke; Dr. Annemarie Schäfer; Dr. Karl Peters; Prof. Dr. Hans Georg von Schnering; Prof. Dr. Heinrich Marsmann

Publisher
John Wiley and Sons
Year
1994
Tongue
English
Weight
271 KB
Volume
106
Category
Article
ISSN
0044-8249

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Bis(2,4,6-tri-tert-butylphenyl)bicyclote
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✍ Ralf Riedel; Dr. Hans-Dieter Hausen; Prof. Dr. Ekkehard Fluck 📂 Article 📅 1985 🏛 John Wiley and Sons 🌐 English ⚖ 269 KB 👁 1 views

pounds, presumably oligomers. In glacial acetic acid (CH3C0,H/CH2C12=3 :2, i=40 mA/cm2, T=2OoC, Pt electrode) 17% androstanyl acetate is obtained and 38% androstane is recovered. Remarkable is the selectivity of the oxidation: We found that the 6-(6a), 7-, and 12-acetates are formed in the ratio 35