( Z )-4-(2-Hydroxyanilino)pent-3-en-2-one
✍ Scribed by Fatiha, Benghanem; Saida, Keraghel; Safia, Chahmana; Ali, Ourari; Lydia, Brelot
- Book ID
- 125485452
- Publisher
- International Union of Crystallography
- Year
- 2012
- Tongue
- English
- Weight
- 399 KB
- Volume
- 68
- Category
- Article
- ISSN
- 1600-5368
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📜 SIMILAR VOLUMES
In the structure of the title compound, C 22 H 24 N 2 O 3 , short intermolecular CÐHÁ Á ÁO contacts in¯uence the crystal packing and molecular ladders are formed. Intramolecular NÐHÁ Á ÁO hydrogen bonds make the Z con®guration stable by formation of six-membered rings.
The title compound, C 11 H 13 NO, crystallizes as the Z isomer of the -enamino-ketone. An intramolecular hydrogen-bonding interaction exists between the N-H and C O groups.
Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.060 wR factor = 0.185 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.
## Abstract 4‐(2‐hydroxyphenylamino)‐pent‐3‐en‐2‐one (HPAP) was synthesized and single crystals were grown by the solution growth technique using methanol as a solvent. The crystals having orthorhombic symmetry were characterized by single crystal XRD, FTIR spectroscopy, NMR spectroscopy, TGA, DSC