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Growth and characterization of 4-(2-hydroxyphenylamino)-pent-3-en-2-one single crystals

✍ Scribed by B. B. Parekh; D. H. Purohit; P. Sagayaraj; H. S. Joshi; M. J. Joshi


Book ID
102121761
Publisher
John Wiley and Sons
Year
2007
Tongue
English
Weight
393 KB
Volume
42
Category
Article
ISSN
0232-1300

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✦ Synopsis


Abstract

4‐(2‐hydroxyphenylamino)‐pent‐3‐en‐2‐one (HPAP) was synthesized and single crystals were grown by the solution growth technique using methanol as a solvent. The crystals having orthorhombic symmetry were characterized by single crystal XRD, FTIR spectroscopy, NMR spectroscopy, TGA, DSC and dielectric studies. Very less variation in the value of dielectric constant is found for different frequencies of applied field. The crystals were exhibiting positive photoconductivity and poor NLO responses. (© 2007 WILEY‐VCH Verlag GmbH & Co. KGaA, Weinheim)


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Single-crystal X-ray study T = 293 K Mean '(C±C) = 0.004 A Ê R factor = 0.060 wR factor = 0.185 Data-to-parameter ratio = 13.3 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.