Wide line N.M.R. spectra have been recorded from 90'K for the three dioxonium + salts : n50\*+c104 ; H502+Br and 502 SbC16 . From a second moment analysis in the rigid lattice, external hydrogen bonds are found significantly bent with dOH = 0.991 i for the bromide and 1.009 i for the perchlorate.
โฆ LIBER โฆ
Wide-line 2H n.m.r. study of perdeuterated pyridine imbibed in a premium coal
โ Scribed by Antoni Jurkiewicz; James S. Frye; Gary E. Maciel
- Book ID
- 107756476
- Publisher
- Elsevier Science
- Year
- 1990
- Tongue
- English
- Weight
- 418 KB
- Volume
- 69
- Category
- Article
- ISSN
- 0016-2361
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## Abstract Seven isomeric 4,5,6โtrimethylโ2โoxoโ1,3,2โdioxathians, __cis__โ4โ__trans__โ6โdimethylโ__r__โ2โoxoโ1,3,2โdioxathian and two isomeric 4,5,5,6โtetramethylโ2โoxoโ1,3,2โdioxathians were prepared and their ^1^H n.m.r. spectra analysed. The values of the vicinal coupling constants reported ea