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Vibrational analyses of 1,3-dibenzoyl-4,5-dihydro-1H-imidazole-2-thione and 1,3-dibenzoyl tetrahydropyrimidine-2(1H)-thione by normal coordinate treatment

✍ Scribed by Sedat Gumus; Tom Sundius; Veysel Turan Yilmaz

Book ID
119359967
Publisher
Elsevier Science
Year
2012
Tongue
English
Weight
484 KB
Volume
98
Category
Article
ISSN
1386-1425

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✍ Qun Sun; Xiaoming Zhou; Donald J Kyle πŸ“‚ Article πŸ“… 2001 πŸ› Elsevier Science 🌐 French βš– 113 KB

The solid-phase synthesis of 3,4-dihydro-2(1H)-quinazolinones and 3,4-dihydro-1H-quinazolin-2-thiones is described. Starting from Rink resin, acylation with 4-bromomethyl-3-nitrobenzoic acid and amination with primary amines, reduction with tin chloride and cyclization, the desired 3,4-dihydro-2(1H)