VERY STRONG HYDROGEN BONDING OF PHOSPHATES: X-RAY CRYSTAL STRUCTURES OF 1,2,3-BENZOTRIAZOLIUM DIHYDROGEN PHOSPHATE [C 6 H 4 N 3 H 2+ ][H 2 PO −4 ] AND 1,3-BENZIMIDAZOLIUM DIHYDROGEN PHOSPHATE [C 7 H 5 N 2 H 2+ ][H 2 PO −4 ]
✍ Scribed by Emsley, John; Reza, Naser M.; Dawes, Helen M.; Hursthouse, Michael B.; Kuroda, Reiko
- Book ID
- 126150982
- Publisher
- Informa UK (Taylor & Francis)
- Year
- 1988
- Weight
- 413 KB
- Volume
- 35
- Category
- Article
- ISSN
- 0308-664X
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📜 SIMILAR VOLUMES
To form the radical by oxidation, the substance is shaken with a ten-fold excess of active PbO;! in benzene for 10 min. On rapid removal of the solvent, the reddish-brown solution affords an impure, reddish-brown paramagnetic product.
Two new phases, (C 4 H 12 N 2 )(H 3 O)[(VOPO 4 ) 4 (H 2 O)H 2 PO 4 ] ' 3H 2 O (1) and (C 4 H 12 N 2 )[(VO)(VO 2 ) 2 (H 2 O)(PO 4 ) 2 ] (2) have been synthesized hydrothermally and characterized by single crystal X-ray di4raction, thermogravimetric analysis, and magnetic susceptibility. Compound 1 ha
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