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Pb(H2PO4)4·(C6H5)3PO, Lead(IV) Tetrakis(dihydrogen phosphate) Stablized by Triphenylphosphine Oxide

✍ Scribed by Priv.-Doz. Dr. F. Huber; Dipl.-Chem. M. S. A. El-Meligy

Publisher: John Wiley and Sons
Year: 1968
Tongue: English
Weight: 231 KB
Volume: 7
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.196809462

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✦ Synopsis

To form the radical by oxidation, the substance is shaken with a ten-fold excess of active PbO;! in benzene for 10 min. On rapid removal of the solvent, the reddish-brown solution affords an impure, reddish-brown paramagnetic product.

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