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Versatile Reagent for Reduction of Azides to Amines

โœ Scribed by Pal, Bikash; Jaisankar, Parasuraman; Giri, Venkatachalam S.

Book ID
115533367
Publisher
Taylor and Francis Group
Year
2004
Tongue
English
Weight
144 KB
Volume
34
Category
Article
ISSN
0039-7911

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Chlorotrimethylsilane -sodium iodide reagent (in situ generation of iodotrimethylsilane)in acetonitrile reduces alkyl and aryl/aroyl azides to the corresponding amines/amides in excellent yields under neutral and mild conditions.

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Iodotrimethylsilane: A Mild and Efficient Reagent for the Reduction of Azides to Amines. -An efficient and chemoselective protocol for the reduction of azides using in situ prepared iodotrimethylsilane as a reducing agent is reported. The corresponding amines are formed in excellent yields. -

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