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Trichloro­[tris­(3-mesitylpyrazol-1-yl)borohydrido]titanium dichloro­methane disolvate

✍ Scribed by Michiue, Kenji ;Steele, Ian ;Casagrande, Osvaldo L. ;Jordan, Richard F.

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
133 KB
Volume
62
Category
Article
ISSN
1600-5368

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In the title Ti III complex, [Ti(C 36 H 40 BN 6 )Cl 2 (C 12 H 14 N 2 )]Á-C 7 H 8 , the Ti atom is coordinated in a distorted octahedral geometry by three N atoms that are constrained to a facial arrangement by the Tp Ms\* ligand [Tp Ms\* = HB(3-mesitylpyrazolyl) 2 (5-mesitylpyrazolyl)], by two mutua

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Single-crystal X-ray study T = 200 K Mean (C-C) = 0.007 A R factor = 0.071 wR factor = 0.162 Data-to-parameter ratio = 15.2 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

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In the title complex, [CuCl~2~(C~31~H~28~N~6~)]·0.5C~2~H~3~N, the Cu^2+^ atom is coordinated in a distorted square-pyramidal geometry by three N atoms from the pyrazolyl groups of the tripodal ligand, and by two chloride anions.