𝔖 Bobbio Scriptorium
✦   LIBER   ✦

(SR)-5-(2,6-Dichloro­phen­yl)-3-(2-naphth­yl)-1-phenyl-2-pyrazoline trichloro­methane hemisolvate

✍ Scribed by Lu, Zhi-Ke ;Xie, Bi-Xia ;Huang, Peng-Mian

Publisher
International Union of Crystallography
Year
2006
Tongue
English
Weight
107 KB
Volume
63
Category
Article
ISSN
1600-5368

No coin nor oath required. For personal study only.

✦ Synopsis

Single-crystal X-ray study T = 294 K Mean (C-C) = 0.005 A Disorder in solvent or counterion R factor = 0.051 wR factor = 0.138 Data-to-parameter ratio = 12.1 For details of how these key indicators were automatically derived from the article, see http://journals.iucr.org/e.

📜 SIMILAR VOLUMES

1-Acetyl-5-(2,6-dichloro­phen­yl)-3-(2-n
1-Acetyl-5-(2,6-dichloro­phen­yl)-3-(2-naphth­yl)-2-pyrazoline
✍ Lu, Zhi-Ke ;Li, Shen ;Huang, Peng-Mian 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 163 KB

In the title compound, C 21 H 16 Cl 2 N 2 O, the pendant benzene ring and the naphthalene ring system make dihedral angles of 82.9 (3) and 6.7 (3) , respectively, with the central pyrazoline ring.

3-(4-Bromo­phen­yl)-5-(2-chlorophen­yl)-
3-(4-Bromo­phen­yl)-5-(2-chlorophen­yl)-1-phenyl-2-pyrazoline
✍ Guo, Huan-Mei ;Jian, Fang-Fang ;Wang, Lei ;Li, Li-Min ;Wu, Qian 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 163 KB

In the title compound, C 21 H 16 BrClN 2 , the pyrazolinyl ring is approximately perpendicular to the chlorophenyl ring, with a dihedral angle of 82.08 .

1-(2-Chloro­phen­yl)-3-(2,6-dichloro­ben
1-(2-Chloro­phen­yl)-3-(2,6-dichloro­benzo­yl)thio­urea toluene hemisolvate
✍ Khawar Rauf, M. ;Badshah, Amin ;Bolte, Michael ;Imtiaz-ud-Din, 📂 Article 📅 2006 🏛 International Union of Crystallography 🌐 English ⚖ 121 KB

In the title compound, C 14 H 9 Cl 3 N 2 OSÁ0.5C 7 H 8 , the toluene molecule is disordered over a centre of inversion. The dihedral angle formed by the two benzene ring planes is 2.26(8) .

3-(4-Bromo­phen­yl)-5-(4-chloro­phen­yl)
3-(4-Bromo­phen­yl)-5-(4-chloro­phen­yl)-1-phenyl-2-pyrazoline
✍ Guo, Huan-Mei ;Jian, Fang-Fang ;Xiao, Hai-Lian ;Sun, Xiao-Zheng ;Li, Yu-Feng 📂 Article 📅 2007 🏛 International Union of Crystallography 🌐 English ⚖ 152 KB

In the title structure, C~21~H~16~BrClN~2~, the pyrazoline ring is approximately coplanar with the __N__-substituted phenyl ring. The dihedral angles formed by the pyrazoline ring with the 4-chlorophenyl and 4-bromophenyl rings are 78.82 and 10.9°, respectively.