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Transition-Metal-Free Alkynylation of Aryl Chlorides

✍ Scribed by Truong, Thanh; Daugulis, Olafs

Book ID
120523194
Publisher
American Chemical Society
Year
2011
Tongue
English
Weight
790 KB
Volume
13
Category
Article
ISSN
1523-7060

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was concentrated under reduced pressure and purified by column chromatography (cyclohexane/ethyl acetate as eluant). Acetone (3 mL, 0.9 m) was added to the reaction mixtures involving esters 1 b,c and the amount of TEA was increased to 0.1m.

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