Photo-Cross-Coupling Reaction of Electron-Rich Aryl Chlorides and Aryl Esters with Alkynes: A Metal-Free Alkynylation
β Scribed by Stefano Protti; Maurizio Fagnoni; Angelo Albini
- Publisher
- John Wiley and Sons
- Year
- 2005
- Tongue
- English
- Weight
- 121 KB
- Volume
- 117
- Category
- Article
- ISSN
- 0044-8249
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π SIMILAR VOLUMES
was concentrated under reduced pressure and purified by column chromatography (cyclohexane/ethyl acetate as eluant). Acetone (3 mL, 0.9 m) was added to the reaction mixtures involving esters 1 b,c and the amount of TEA was increased to 0.1m.
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