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Photo-Cross-Coupling Reaction of Electron-Rich Aryl Chlorides and Aryl Esters with Alkynes: A Metal-Free Alkynylation

✍ Scribed by Stefano Protti; Maurizio Fagnoni; Angelo Albini

Publisher: John Wiley and Sons
Year: 2005
Tongue: English
Weight: 122 KB
Volume: 44
Category: Article
ISSN: 0044-8249
DOI: 10.1002/anie.200501541

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✦ Synopsis

was concentrated under reduced pressure and purified by column chromatography (cyclohexane/ethyl acetate as eluant). Acetone (3 mL, 0.9 m) was added to the reaction mixtures involving esters 1 b,c and the amount of TEA was increased to 0.1m.

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