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Traceless Solid-Phase Organic Synthesis

✍ Scribed by Blaney, Paul; Grigg, Ronald; Sridharan, Visuvanathar

Book ID
119995777
Publisher
American Chemical Society
Year
2002
Tongue
English
Weight
456 KB
Volume
102
Category
Article
ISSN
0009-2665

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Traceless Solid-Phase Organic Synthesis
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A photolabile β€˜traceless’ linker for sol
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A photolabile linker based on a thiohydroxamic acid has been shown to be an efficient 'traceless' linker, revealing an aliphatic CH bond on photolysis at 350 nm. Methods for the synthesis, loading and photolytic cleavage of the linker are described.

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Traceless linkers, which enable the attachment of arenes and alkanes to a polymeric support, have received increased attention in recent years. These anchoring groups allow chemical transformations on the polymer-bound molecules, which can be cleaved from the resin leaving no residual functionality