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Total synthesis of (−)-pironetin

✍ Scribed by Hiroyuki Watanabe; Hidenori Watanabe; Takeshi Kitahara

Publisher: Elsevier Science
Year: 1998
Tongue: French
Weight: 214 KB
Volume: 39
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(98)01860-7

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✦ Synopsis

The convergent total synthesis of (-)-pironetin using a chiral building block, (1S,5S,6R)- 5hydroxybicyclo[4.1.0]heptan-2-one 5 is described. Both the dithiane 4 and the epoxide 2 with proper substituents were employed as coupling partners to construct the whole carbon skeleton 15, which was converted to pironetin 1 in a few steps.

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