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Total Synthesis of d,l -Matrine

✍ Scribed by Mandell, Leon.; Singh, K. P.; Gresham, J. T.; Freeman, Walter.

Book ID: 126475460
Publisher: American Chemical Society
Year: 1963
Tongue: English
Weight: 278 KB
Volume: 85
Category: Article
ISSN: 0002-7863
DOI: 10.1021/ja00900a048

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Three different radical reactions were used in a short total synthesis of (±)-matrine (1). Two of the four six-membered rings and four new bonds were created in one radical cascade involving intermolecular addition followed by two successive cyclizations and transfer of a xanthate group.