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Thermodynamic study of the incommensurate phase transitions in crystalline bis(4-chlorophenyl)sulfone

✍ Scribed by Kazuya Saito; Hiroyuki Kamio; Koichi Kikuchi; Isao Ikemoto

Publisher
Elsevier Science
Year
1990
Tongue
English
Weight
476 KB
Volume
163
Category
Article
ISSN
0040-6031

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Heat capacity and an incommensurate phas
Heat capacity and an incommensurate phase transition of crystalline bis(4-chlorophenyl)sulfone
✍ Toshiaki Tanaka; Tooru Atake; Hirokazu Nakayama; Taro Eguchi; Kazuya Saito; Isao πŸ“‚ Article πŸ“… 1994 πŸ› Elsevier Science 🌐 English βš– 250 KB

The heat capacity of crystalline bis(4-chlorophenyl)sulfone was measured from the temperature \(T=14\) to \(T=300 \mathrm{~K}\) by adiabatic calorimetry. An incommensurate phase transition was detected as a second-order type of heat-capacity anomaly at \(T=(148.5 \pm 0.5) \mathrm{K}\). The molar ent

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The kinetics of formation of three dimensional order from the mesophase have been studied for poly(alkyl terephthaloyl bis-(4-oxybenzoate))s with hexa-, hepta-and decamethylene spacers, using differential scanning calorimetry. The rate of transformation and the crystallinity level attained have been