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Thermal decomposition of 1,3,3-trinitroazetidine in the gas phase, solution, and melt

✍ Scribed by V. V. Nedel’ko; B. L. Korsunskii; N. N. Makhova; N. V. Chukanov; T. S. Larikova; I. V. Ovchinnikov; V. A. Tartakovsky

Book ID: 106521375
Publisher: Springer
Year: 2009
Tongue: English
Weight: 236 KB
Volume: 58
Category: Article
ISSN: 1573-9171
DOI: 10.1007/s11172-009-0277-y

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## Abstract The cyclic sulfenic ester 1,2‐oxathiolane (**1**) decomposes thermally (400 – 450 K) exclusively to give acrolein (**3**) __via__ 3‐mercaptopropanal (**2**) by loss of hydrogen sulfide. Isotopic labelling experiments reveal the presence of a 1,2‐oxathiolane‐thietane 1‐oxide equilibrium