𝔖 Bobbio Scriptorium
✦   LIBER   ✦

The use of signal averaging techniques for the quantitation and mass measurement of high molecular weight compounds using fast atom bombardment mass spectrometry

✍ Scribed by L. Grotjahn; L. C. E. Taylor

Publisher
John Wiley and Sons
Year
1985
Tongue
English
Weight
346 KB
Volume
20
Category
Article
ISSN
1076-5174

No coin nor oath required. For personal study only.

✦ Synopsis

The measurement and recording of peak signals at high mass is often ditlicult and susceptible to a large degree of error. Signal averaging of repetitive scans has been used to improve detection limits and aid nominal mass assignment by peak matching. This is illustrated using glucagon as the reference material to determine the mass of the [MH]+ peak in the molecular ion cluster of Vasoactive Intestinal Peptide, and caesium iodide as reference to mass-measure a 13-unit oligonucleotide.

πŸ“œ SIMILAR VOLUMES

The combined use of enzymatic hydrolysis
The combined use of enzymatic hydrolysis and fast atom bombardment mass spectrometry for peptide sequencing
✍ R. Self; A. Parente πŸ“‚ Article πŸ“… 1983 πŸ› John Wiley and Sons 🌐 English βš– 440 KB πŸ‘ 2 views

Oligopeptides subjected to partial enzyme hydrolysis provide mixtures of sub-peptides which optimize amino acid sequence determination by fast atom bombardment mass spectrometry. The digestion mixture can be sampled directly; there is no interference from the enzyme. Complete sequences were obtained

ChemInform Abstract: The Analysis of Str
ChemInform Abstract: The Analysis of Structure and Function of Organic Compounds Using Fast Atom Bombardment Mass Spectrometry
✍ Mitsuo Takayama πŸ“‚ Article πŸ“… 2010 πŸ› John Wiley and Sons βš– 24 KB πŸ‘ 1 views

## Abstract ChemInform is a weekly Abstracting Service, delivering concise information at a glance that was extracted from about 100 leading journals. To access a ChemInform Abstract of an article which was published elsewhere, please select a β€œFull Text” option. The original article is trackable v

Fast atom bombardment mass spectrometry
Fast atom bombardment mass spectrometry for the determination of the molecular weight distribution of poly(ethylene glycols) and their derivatives
✍ Roberta Seraglia; Pietro Traldi; Raniero Mendichi; Luciana Sartore; Oddone Schia πŸ“‚ Article πŸ“… 1992 πŸ› Elsevier Science 🌐 English βš– 426 KB

A fast atom bombardment mass spectrometrlc method for the characterlzatlon of polfiethylene glycols) (PEGS) and monomethoxy(polyethylene glycols) (MMPEGs) and theu denvatlves IS described This method, m comparison with the classIcal rheologxal measurements, offers the advantage of gwmg the abundance

Study of C2+2X- Organic Salts by Simulta
Study of C2+2X- Organic Salts by Simultaneous Use of Fast Atom Bombardment Mass Spectrometry and Tandem Mass Spectrometry. Chemical Reactivity in the Gaseous Phase
✍ Calas, MichΓ¨le; Cordina, GΓ©rard; Gilles, Isabelle; Aubagnac, Jean-Louis πŸ“‚ Article πŸ“… 1997 πŸ› John Wiley and Sons 🌐 English βš– 287 KB πŸ‘ 2 views

The observed fragmentations in collisionally activated dissociation (CAD) spectra of CX' adduct ions formed in the fast atom bombardment (FAB) mass spectra of C2'2X-bisammonium salts are the same as those previously put forward to account for the FAB mass spectra of these compounds. Thus, substituti

Syntheses of deuterated leu-enkephalins
Syntheses of deuterated leu-enkephalins and their use as internal standards for the quantification of leu-enkephalin by fast atom bombardment mass spectrometry
✍ Dr. E. Benfenati; G. Icardi; S. Chen; R. Fanelli πŸ“‚ Article πŸ“… 1990 πŸ› John Wiley and Sons 🌐 French βš– 348 KB

## Abstract We have developed a synthetic method for the preparation of di‐ and pentadeuterated leu‐enkephalin (LE), Tyr‐Gly‐Gly‐Phe‐Leu, by proton‐deuterium exchange using CF~3~COO^2^H. Four to six deuterium atoms are introduced using a reaction temperature of 120Β°C and if 5% of ^2^H~2~O is added