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The synthesis of14C- and3H-labeled glycerol ethers

โœ Scribed by Edward O. Oswald; Claude Piantadosi; Carl E. Anderson; Fred Snyder

Book ID
112770631
Publisher
Springer-Verlag
Year
1966
Tongue
English
Weight
448 KB
Volume
1
Category
Article
ISSN
0024-4201

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## Abstract The preparation of [^3^H]Sch 727965 from unlabeled compound and tritiated water was base catalyzed. Diethyl [^13^C~3~]malonate was used to prepare [^13^C~3~]Sch 727965 in five steps in 21.8% overall yield. In a similar manner, [^14^C]Sch 727965 was prepared in five steps from diethyl [2