The synthesis of [ring-U-14C] DDD from [ring-U-14C] DDT using rat liver homogenate
✍ Scribed by S. C. Fawcett; L. J. King; P. I. Stanley; P. J. Bunyan
- Publisher
- John Wiley and Sons
- Year
- 1981
- Tongue
- French
- Weight
- 164 KB
- Volume
- 18
- Category
- Article
- ISSN
- 0022-2135
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✦ Synopsis
Abstract
1,1‐Di[ring‐U‐^14^C] (4‐chlorophenyl)‐2,2‐dichloroethane ([^14^C] DDD) was prepared by the anaerobic incubation of 1,1‐di[ring‐U‐^14^C] (4‐chlorophenyl)‐2,2,2‐trichloroethane ([^14^C] DDT) with homogenised rat liver in buffer. This gave a good yield of DDD which was purified chromatographically. The overall recovery of 99.5% pure DDD was 68%.
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