𝔖 Bobbio Scriptorium
✦   LIBER   ✦

The Synthesis of Methylamine-C 14 and Diazomethane-C 14 1

✍ Scribed by Heard, R. D. H.; Jamieson, J. R.; Solomon, S.


Book ID
126131175
Publisher
American Chemical Society
Year
1951
Tongue
English
Weight
309 KB
Volume
73
Category
Article
ISSN
0002-7863

No coin nor oath required. For personal study only.


📜 SIMILAR VOLUMES


Synthesis of daunorubicin-14-14C and adr
✍ C. Rolland Chen; Mary Tan Fon; Alan N. Fujiwara; David W. Henry; Morris A. Leaff 📂 Article 📅 1978 🏛 John Wiley and Sons 🌐 French ⚖ 275 KB

## Abstract Reaction of adriamycinone with excess ^14^CH~3~Mgl and periodate cleavage of the resulting glycol (5) affords daunomycinone‐14‐^14^C (6). Bromination and hydrolysis of 6 gives adriamycinone‐14‐^14^C (8). Coupling of 6 and the 14‐0‐p‐anisyldiphenyl‐methyl derivative (9) with 1‐chloro‐3‐N

Synthesis of carbon-14 labeled 1,4-benzo
✍ Richard S. P. Hsi 📂 Article 📅 1974 🏛 John Wiley and Sons 🌐 French ⚖ 287 KB 👁 1 views

## Abstract Diazepam‐^14^C and demethyldiazepam‐^14^C are synthesized from glycine‐1‐^14^C. Addition of diketene to diazepam‐^14^C leads to ketazolam‐^14^C. The reaction conditions for the formation of ketazolam from diazepam is studied using high‐pressure liquid chromatography in conjunction with