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The synthesis of deuterium labeled T-2 toxin

✍ Scribed by Dennis P. Michaud; B. L. Karger; Paul Vouros


Publisher
John Wiley and Sons
Year
1988
Tongue
French
Weight
175 KB
Volume
25
Category
Article
ISSN
0022-2135

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✦ Synopsis


m m R Y we report the synthesis of isotopically pure trideuteriated T-2 toxin, a useful internal standard for mycotoxin analysis. Peracetylation of K F 2 toxin with hewdeuteriated acetic anhydride, follorJed by selective hydrolysis of the C-3 acetate afforded the desired caapound in good yield.


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