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The synthesis of 6-deoxy-6-18F-α-D-galactopyranose (XXII)

✍ Scribed by David R. Christman; Zlata Orhanovic; Walton W. Shreeve; Alfred P. Wolf

Publisher
John Wiley and Sons
Year
1977
Tongue
French
Weight
204 KB
Volume
13
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

The synthesis of 6‐deoxy‐6–^18^F‐α‐D‐galactopyranose from the 6‐tosyl‐1,2:3,4‐di‐O‐isopropylidene derivative, using tetraethyl‐ammonium fluoride‐^18^F is described. The synthesis requires 4–4 1/2 hours for completion. The radiochemical yield (activity in compound/starting activity. corrected for decay) is about 15%. Thus 3–4% of the starting ^18^F^–^ activity is present at the time of delivery, in approximately 0.2 mg of product.

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