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The Synthesis and Reactions of 5,5-Difluorotetrachlorocyclopentadiene 1

✍ Scribed by McBee, E. T.; Smith, D. K.; Ungnade, H. E.


Book ID
118016366
Publisher
American Chemical Society
Year
1955
Tongue
English
Weight
407 KB
Volume
77
Category
Article
ISSN
0002-7863

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Synthesis and reactions of 5,5-dinitroba
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Nitration of barbituric acid at 40Β°C gave the previously unknown 5,5-dinitrobarbituric acid (3), which readily underwent hydrolysis to dinitroacetylurea (5), which in turn could be hydrolysed in basic media to the potassium salt of dinitromethane. Alloxane was prepared in a one step procedure by the