✦ LIBER ✦

The synthesis and characterization of organoimido- Re(V) complexes. The x-ray crystal structures of [ReCl(NC6H4Me-4) (OMe)(tBuNC)2(PPh3)][BPh4] and [ReCl2(NC6H4Me-4)(PPh3)4-ClC6H4(O)CNNCHPh-O,N]

✍ Scribed by Mustafa T. Ahmet; Brian Coutinho; Dilworth Jonathan R.; John R. Miller; Suzanne J. Parrott; Yifan Zheng

Publisher: Elsevier Science
Year: 1996
Tongue: English
Weight: 706 KB
Volume: 15
Category: Article
ISSN: 0277-5387
DOI: 10.1016/0277-5387(78)00447-7

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## Abstract The preparation of a family of dinuclear monocyclopentadienyl imidoniobium and ‐tantalum complexes was achieved by two different synthetic routes. The diimido complexes [{M(Cp′)Cl~2~}~2~(μ‐1,__i__‐NC~6~H~4~N)] [Cp′ = η^5^‐C~5~H~4~SiMe~3~, M = Nb, __i__ = 4 (1); Cp′ = η^5^‐C~5~H~4~SiMe~3