๐”– Bobbio Scriptorium
โœฆ   LIBER   โœฆ

The reduction of aromatic nitro groups on solid supports using sodium hydrosulfite (Na2S2O4)

โœ Scribed by Randall A Scheuerman; David Tumelty


Publisher
Elsevier Science
Year
2000
Tongue
French
Weight
341 KB
Volume
41
Category
Article
ISSN
0040-4039

No coin nor oath required. For personal study only.

โœฆ Synopsis


An improved method for reducing aromatic nitro compounds on solid-phase supports using sodium hydrosulยฎte is presented. Conditions have been optimized to enable the use of this reagent for reductions on both polyethyleneglycol-polystyrene (PEG) resins and traditional polystyrene (PS) resins.


๐Ÿ“œ SIMILAR VOLUMES


Facile reduction of aromatic nitro/azido
โœ Ahmed Kamal; K.Laxma Reddy; V. Devaiah; G.Suresh Kumar Reddy ๐Ÿ“‚ Article ๐Ÿ“… 2003 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 355 KB

An efficient and mild method for the reduction of aromatic nitro and azido groups on solid support using Al/NiCl 2 โ€ข6H 2 O and Al/NH 4 Cl is described. This solid phase reduction technique has been applied towards the synthesis of DNA binding pyrrolo[2,1-c][1,4]benzodiazepine antitumour antibiotics.

A new method for the mild and selective
โœ Anitha Hari; Benjamin L. Miller ๐Ÿ“‚ Article ๐Ÿ“… 1999 ๐Ÿ› Elsevier Science ๐ŸŒ French โš– 164 KB

An efficient method for the solid-phase reduction of aryl nitro groups to anilines is describedโ€ข Among the several reagents tried, chromium chloride was found to be most effective for this reaction. For the substrates examined, reduction occurs in high yield regardless of the substitution pattern on