✦ LIBER ✦

The preparation of uniformly labeled cyclohexylamine and cyclamate

✍ Scribed by A. Alter; J. C. Forman

Publisher: John Wiley and Sons
Year: 1968
Tongue: French
Weight: 228 KB
Volume: 4
Category: Article
ISSN: 0022-2135
DOI: 10.1002/jlcr.2590040406

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✦ Synopsis

Aniline uniformly labeled with 14C was reduced, in the presence of Rhodium on Alumina catalyst, to cyclohexylamine. The cyclohexylamine was converted to uniformly labeled sodium cyclamate.

The overall radiochemical yield was 34 %.

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