We have investigated the ct-acetoxylation of benzylamine derivatives 4 from substituted benzylphthalimide 3 using NBWAcONdAcOH in chlorobenzene at reflux.
The preparation of mono- and di-benzylamines
โ Scribed by Phillips, M. A.
- Publisher
- Wiley (John Wiley & Sons)
- Year
- 1947
- Weight
- 131 KB
- Volume
- 66
- Category
- Article
- ISSN
- 0368-4075
No coin nor oath required. For personal study only.
โฆ Synopsis
Abstract
The preparation of monoโ and dibenzylamines from benzyl halides and acetamide and benzaldehyde is compared with a B.I.O.S. method and the experimental procedure described.
๐ SIMILAR VOLUMES
## Abstract The preparation of the unsymmetrically isotopeโlabelled title compounds was achieved in pure form for the first time. While monoโ^15^Nโcyanogen is available in a twoโstepโsynthesis, the preparation of monoโ^13^Cโcyanogen requires five steps, the last step in both cases being the dehydra
The general principles and practical aspects of preparative high-performance liquid chromatography (l.c.) of mono- and di-saccharides, sugars acids, lactones, and N-acetylated amino sugar derivatives are described. Milligram to gram quantities of these carbohydrates were isolated on semi-preparative