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The preparation of chloral-1,2-14C hydrate

✍ Scribed by L. E. Weaner; G. L. Burghard; D. W. Blackburn; W. L. Mendelson

Publisher
John Wiley and Sons
Year
1977
Tongue
French
Weight
187 KB
Volume
13
Category
Article
ISSN
0022-2135

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✦ Synopsis

Abstract

Chloral‐1,2‐^14^C hydrate was prepared by direct chlorination of labeled acetaldehyde in an overall 47% radiochemical yield. The reaction was carried out without a catalyst by heating at one temperature in a single stage reaction. No lower chloroacetaldehydes were detected.

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