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The preparation of a new series of α, α-disubstituted vinyl monomers

✍ Scribed by R. Devarajan; T. Balakrishnan

Book ID: 104704406
Publisher: Springer
Year: 1979
Tongue: English
Weight: 136 KB
Volume: 1
Category: Article
ISSN: 0170-0839
DOI: 10.1007/bf00284416

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## Abstract The two‐step alkylation of phenyl prop‐2‐enyl sulfone (1) with protected ω‐bromoalkanols and 1‐iodoalkanes (→3; see __Scheme 1__) followed by a Pd‐catalyzed desulfonylation with LiBH~4~ affords a 96:4 mixture of vinylbranched, protected alcohols and corresponding ethylidene‐branched iso