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The Preparation of 3,4-bis-(3′-Methyl-4′-hydroxy-5′-allylphenyl)-2,4-hexadiene

✍ Scribed by Weiss, Philip.; Niederl, Joseph B.


Book ID
126824676
Publisher
American Chemical Society
Year
1949
Tongue
English
Weight
223 KB
Volume
71
Category
Article
ISSN
0002-7863

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Methyl 4-(4-hydroxy-3-methoxyphenyl)-6-m
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The title compound, C 14 H 16 N 2 O 4 S, was synthesized by the reaction of 4-hydroxy-3-methoxybenzaldehyde, thiourea and methyl 3-oxobutanoate in ethanol under reflux. The crystal structure is stabilized mainly through intermolecular N-HÁ Á ÁS and O-HÁ Á ÁO hydrogen bonds. The tetrahydropyrimidin-2