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The first synthesis of the epoxide-containing macrolactone nucleus of oximidine I

✍ Scribed by Joanne E. Harvey; Steven A. Raw; Richard J.K. Taylor

Book ID: 104254340
Publisher: Elsevier Science
Year: 2003
Tongue: French
Weight: 191 KB
Volume: 44
Category: Article
ISSN: 0040-4039
DOI: 10.1016/s0040-4039(03)01775-1

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✦ Synopsis

A synthesis of the epoxydiene-containing macrolide nucleus of oximidine I is reported, starting from commercially available 3-butyn-1-ol. The key macrocyclisation step is achieved using Horner-Wadsworth-Emmons methodology in the presence of an epoxide.

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