The crystal structure of t-Bu2Si(OH)F. A cyclic hydrogen-bonded tetramer
โ Scribed by Nabeel H. Buttrus; Colin Eaborn; P.B. Hitchcock; Anil K. Saxena
- Publisher
- Elsevier Science
- Year
- 1985
- Tongue
- English
- Weight
- 259 KB
- Volume
- 287
- Category
- Article
- ISSN
- 0022-328X
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A single-crystal, X-ray diffraction study was performed on a nonalkenic, cyclic trimer (C,,H,sO,, 4) of levoglucosenone, in order to confirm its chemical structure. Crystals of 4 are orthorhombic, with unit-cell parameters of a = 792.20, b = 1874.35, c = 2383.02 pm, space group P2,2,2,, and z = 8. T