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The crystal structure of [4,4,4-trifluoro-3,3-dihydroxy-1-phenyl-1-butanonato(2–)-O,O',0'']tris(p-tolyl)antimony(V)–1,2-dichloroethane (2/1)

✍ Scribed by Ebina, F. ;Ouchi, A. ;Yoshino, Y. ;Sato, S. ;Saito, Y.


Book ID
114525111
Publisher
International Union of Crystallography
Year
1978
Weight
388 KB
Volume
34
Category
Article
ISSN
0567-7408

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Crystal and molecular structure of 1,3-d
✍ Consuelo Bellver; Amparo López-Castro; José Fernández-Bolaños Guzmán 📂 Article 📅 1991 🏛 Elsevier Science 🌐 English ⚖ 390 KB

The title compound was prepared by heating 1 under reflux with 2,2-dimethoxypropane in 1 ,Zdimethoxyethane'. Neutral conditions were used in order to avoid the formation of anhydro rings2T3. X-Ray analysis confirmed the structure 2, for which the bond lengths and angles are shown in Table If and a