✦ LIBER ✦

Crystal and molecular structure of 1,3-dihydro-4-(3,4-O-isopropylidene-d-arabino-tetritol-1-yl)-3-methyl-1-p-tolyl-2H-imidazole-2- thione

✍ Scribed by Consuelo Bellver; Amparo López-Castro; José Fernández-Bolaños Guzmán

Publisher: Elsevier Science
Year: 1991
Tongue: English
Weight: 390 KB
Volume: 209
Category: Article
ISSN: 0008-6215
DOI: 10.1016/0008-6215(91)80163-h

No coin nor oath required. For personal study only.

✦ Synopsis

The title compound was prepared by heating 1 under reflux with 2,2-dimethoxypropane in 1 ,Zdimethoxyethane'.

Neutral conditions were used in order to avoid the formation of anhydro rings2T3. X-Ray analysis confirmed the structure 2, for which the bond lengths and angles are shown in Table If and a stereo view of the molecule with the atomic numbering is shown in Fig. 1.

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