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The Assignment of the Absolute Configuration of 1,2-Diols by Low-Temperature NMR of a Single MPA Derivative

✍ Scribed by Freire, Félix; Seco, José Manuel; Quiñoá, Emilio; Riguera, Ricardo


Book ID
127126663
Publisher
American Chemical Society
Year
2005
Tongue
English
Weight
143 KB
Volume
7
Category
Article
ISSN
1523-7060

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NMR determination of the absolute config
✍ Hiroki Fukui; Yukiharu Fukushi; Satoshi Tahara 📂 Article 📅 2003 🏛 Elsevier Science 🌐 French ⚖ 218 KB

Each of the chiral 1,2-and 1,3-diols examined was derivatized exclusively to a single diastereomeric acetal by the use of a new axially chiral reagent, 2%-methoxy-1,1%-binaphthalene-8-carbaldehyde (MBC). The absolute configuration of the original 1,2-and 1,3-diols was determined by the NOE correlati